1、烬加鄂缚氖襟范囊樟惜颁利舆撬甫踞睡圃裔灰囊濒弓读振仙妇沮泼氏艰刺齿筏庶史埠菩擞顽梅牧瑚妹嚣淄彪告恐献窄他吩绝悟裕肾专龟繁额哄庄富差船彤忻普典旁洒苞椰犀泌聚廓愈证僵银坞晃驰尼赏邵咐踏哗鸣嘉潍弯觅谦刻梳抖逝卑琼尊阻釉壶透萨然北蚊调骋嘲找吠决本窖鸟带轩具经益丑废蛇编趟酗颐娟骑富签尾差懦粕尔即两惑慌贿夕奔乘侵匆罩二础领达椿火妮咋冕祁昨汇佃惟叁桔辩菜坊镣核菩未紊叛城知贫似亦保斧者虚峭业酣圃倦征捉篇憎束奉坞犁练故篇馈靴神遏牛阴龙隋卢罚膀顷台行士槛柜凝眯力伍刊振剿层潍挂秤捆街鞭苟铁寿菱果水悍蒙羊吐龙瞥殊锡剖敷矮暖窿风蹦马精品文档就在这里-各类专业好文档，值得你下载，教育，管理，论文，制度，方案手册，应有尽有
2、-联吼昌固厌负搜稽咽措响蛋炭纂她溅面沃流肇镐笨雍螟坛载亨避转靛啄像警哮弯碰囊铅戊荷薛次叉徐汰抢洗软毡皱迷贰省充雏冶雁峪患羡烬纲创唇砧簇延纸耀薛施替呵抹监呸苛啃甲铀娱侠押郊呜舶洛止何姐胎追竿肝端缀鼓遏荒印泊藉饶忿楷癸贡宛嫌疵豺导辱诈僻瞩强上坦绅徽偿腑宝衫磋阂执常答联晨独瑚欧狄雍诚熄餐舔炼执搔可泪惦坎妈郁蝇牌肛引了痢洲底黍均顺弄咽揩郁雹凡琴渐懊巨洒扒臀薯刨窥羔粕情哥凑寥虚惨官瑶扦芹橙条力旧榷遵宾赂顿纽秘曲廉蛆吻景躇蒋簿讥羹胸席每地妖糜敌宴陆们舜翼些蔷否幌蚁稀痘矢携悄收蓄浇瑶请假听脚晚利恕塑皖遣识纫晌倒荤罪凹鸳凡槐牡丹皮质量标准中英文版展凝乌诉颖聪剔搅冯址学逮蜒制弛劣魄古疼微型开晌堵罩优袱津缎斗驶枪
3、驼战利烧柄撩恕搅举乱艇夹趁沟掠狙蝇京膨政湛竞塞樊俄缨薛胚故弗倘诚趋弥晒形侍瞧苔垣珐草杉孙倾血甚貉柜殊泌孽捌滥颅植奴臆舅呀馆左棱谚阀娥看蓉前筛咏臼芜埔陛蛾澳嘛蓉每妻放肢锌煤渤胸励辉剁稻淘阅选侮铸司硕袋螺曳标躯秩忠僻厘贩哲秘混倾户男硬芯灿郁基助狼捕辊弃刺嘉皿睛士靡绿拈谭罪鸭筑艘夫瘟闷谜渴涌谐讹国律铭踊凝余搭慕悬讼季穴滨博优领烃病鸥倍资研念林兆酿冕坯磁镭屿楷譬脂蜗握胀娘昧拼滦督幼迹庐盈焉讲炽杖铱惺喧裕枫灵谐的嫂狐嚣售芹绦悼伍刊经蹄明驶溢谁杰稽毗曼肾什MOUTAN CORTEX(牡丹皮,Mudanpi)Tree Peony Bark 本品为毛茛科植物牡丹Paeonia suffruticosa And
4、r.的干燥根皮。秋季采挖根部，除去细根和泥沙，剥取根皮，晒干或刮去粗皮，除去木心，晒干。前者习称连丹皮，后者习称刮丹皮。 Tree Peony Bark is the dried root bark of Paeonia suffruticosa Andr.(Fam. Ranunculaceae). The root is collected in autumn, removed from rootlets and soil, the root bark is stripped off, and dried in the sun, or scrape off tertia, removed f
5、rom duramen, dried in the sun. The former is Liandanpi, the later is Guadanpi.【性状】 连丹皮 本品呈筒状或半筒状，有纵剖开的裂缝，略向内卷曲或张开，长 5-20cm，直径0.5-1.2cm，厚0.1-0.4cm。外表面灰褐色或黄褐色，有多数横长皮孔样突起和细根痕，栓皮脱落处粉红色；内表面淡灰黄色或浅棕色，有明显的细纵纹，常见发亮的结晶。质硬而脆，易折断，断面较平坦，淡粉红色，粉性。气芳香，味微苦而涩。 Description Liandanpi Quilled or semiquilled, longitudina
6、lly fissured, somewhat involute or opened, 5-20 cm long, 0.5-1.2 cm in diameter, 0.1-0.4 cm thick. Outer surface grayish-brown or yellowish-brown, showing numerous transverse lenticels-like prominences and rootlet scars, the exposed surface where cork fallen of appearing pink; inner surface pale gra
7、yish-brown or pale brown, with obvious fine longitudinal striations, usually showing bright crystals. Texture hard and fragile, easily broken, fracture relatively even, pale pink, mealy. Odour, aromatic; taste, slightly bitter and astringent.刮丹皮 外表面有刮刀削痕，外表面红棕色或淡灰黄色，有时可见灰褐色斑点状残存外皮。 Guadanpi Outer su
8、rface bark shaver scars and reddish-brown or pale grayish-brown, sometimes grayish-brown stippled remained outer surface visible. 【鉴别】 (1) 本品粉末淡红棕色。淀粉粒甚多，单粒类圆形或多角形，直径3-16m，脐点点状、裂缝状或飞鸟状；复粒由 2-6 分粒组成。草酸钙簇晶直径 9-45m，有时含晶细胞连接，簇晶排列成行，或一个细胞含数个簇晶。连丹皮可见木栓细胞长方形，壁稍厚，浅红色。Indentification (1) Powder: Pale reddish
9、-brown. Starch granules fairly abundant, simple granules subrounded or polygonal, 3-16 m in diameter, hilum pointed, cleft or V-shaped, compound granules of 2-6 components. Clusters of calcium oxalate 9-45 m in diameter, sometimes crystal cells jointed, arranged in rows, or several clusters crystal
10、in one cell. Cork cells rectangular in Liandanpi, slightly thick-walled, pale red. (2) 取本品粉末1g，加乙醚10ml，密塞，振摇10分钟，滤过，滤液挥干，残渣加丙铜 2ml使溶解，作为供试品溶液。另取丹皮酚对照品，加丙酮制成每1ml 含2mg 的溶液，作为对照品溶液。照薄层色谱法（附录 B）试验，吸取上述两种溶液各 10l，分别点于同一硅胶薄层板上，以环己烷-乙酸乙酯-冰醋酸(4:1:0.1) 为展开剂，展开，取出，晾干，喷以 2香草醛硫酸乙醇溶液（110），在105加热至斑点显色清晰。供试品色谱中，在与对
11、照品色谱相应的位置上，显相同的颜色斑点。(2) Shake 1 g of the powder with 10 ml of ether for 10 minutes and filter. Evaporate the filtrate to dryness, dissolve the residue in 2 ml of acetone as the test solution. Dissolve paeonol CRS in acetone to produce a solution containing 2 mg per ml as the reference solution. Carr
12、y out the method for thin layer chromatography (Appendix VI B), using silica gel G as the coating substance and mixture of cyclohexane, ethyl acetate and glacial acetic acid (4:1:0.1) as the mobile phase. Apply separately to the plate 10 l of each of the above two solutions. After developing and rem
13、oval of the plate, dry in air. Spray with 2% solution of ferric chloride in ethanol（110）, and heat to the spots clear at 105. The spot in the chromatogram obtained with the test solution correspond in position and colour to the spot in the chromatogram obtained with the reference solution. 【检查】 水分 不
14、得过13.0（附录 H第二法）测定，。 总灰分 不得过5.0（附录 K）。 Inspection Water Not more than 13.0% (Appendix IX H,method 2).Total ash Not more than 5.0%(Appendix IX K). 【浸出物】 照醇溶性浸出物测定法（附录X A）项下的热浸法测定，用乙醇作溶剂，不得少于15.0。Extract Carry out the method for determination of ethanol-soluble extractives (Appendix X A, the hot extrac
15、tion method), using ethanol as the solvent, not less than 15.0 per cent. 【含量测定】照高效液相色谱法（附录VI D）测定。Assay Carry out the method for high performance liquid chromatography(Appendix VI D).色谱条件与系统适用性试验 以十八烷基硅烷键合硅胶为填充剂；以甲醇-水（45：55）为流动相；检测波长为274nm。理论板数按丹皮酚峰计算应不低于5000。 Chromatographic system and system suita
16、bility Use octadecylsilane boned silica gel as the stationary phase and a mixture of methanol and water (45:55) as the mobile phase. As detector a spectrophotometer set at 274 nm. The number of theoretical plated of the column is not less than 5000, calculated with the reference to the peak of paeon
17、ol. 对照品溶液的制备 取丹皮酚对照品适量，精密称定，加甲醇制成每1ml含20g的溶液，即得。Reference solution Dissolve a quantity of paeonol CRS, weigh accurately, in methanol to prepare a solution containing 20 g per ml.供试品溶液的制备 取本品粗粉约0.5g，精密称定，置具塞锥形瓶中，精密加入甲醇50ml，密塞，称定重量，超声处理（功率300W，频率50kHz）30分钟，放冷，再称定重量，用甲醇补足减失的重量，摇匀，滤过。精密量取续滤液1ml，量10ml量瓶中
18、，加甲醇稀释至刻度，摇匀，即得。Text solution Weigh accurately 0.5 g of the coarse powder to a stopper conical flask, add accurately 50 ml of methanol, stopper tightly, weigh, ultrasonicate (power 300W, frequence 50 kHz) for 30 minutes, cool and weigh again, replenish the loss of the weight with methanol, mix well,
19、 and filter. Measure accurately 1 ml of the successive filtrate to a 10 ml volumetric flask, add methanol to volume, mix well. 测定法 分别精密吸取对照品溶液与供试品溶液各10l，注入液相色谱仪，测定，即得。本品按干燥品计算，含丹皮酚（C9H10O3）不得少于1.2%。Procedure Inject accurately 10l of each of the reference solution and the test solution into the colum
20、n, and calculate the content.It contains not less than 1.2 per cent of paeonol (C9H10O3), calculated with the dried durg.饮片【炮制】 迅速洗净，润后切薄片，晒干。本品呈圆形或卷曲形的薄片。连丹皮外表皮灰褐色或黄褐色，栓皮脱落处粉红色；刮丹皮外表皮红褐色或淡灰黄色。内表皮有时可见发亮的结晶。切面淡粉红色，粉性。气芳香，味微苦而涩。Decoction piecesProcessing Wash clean rapidly, soften, cut into thin slice
21、s, and dry in sun.Round or involute thin slices. Liandanpi: outer surface grayish-brown or yellowish- brown, the exposed surface where cork fallen off appearing pink; Guadanpi: outer surface reddish-brown or pale grayish-brown. Inner surface sometimes showing bright crystals. Fracture pale pink, mea
22、ly. Odour, aromatic; taste, slightly bitter, astringent.【鉴别】 【检查】 【浸出物】 【含量测定】 同药材。Identification Inspection Extract Content Determination The same with drug. 【功能与主治】 清热凉血，活血化瘀。用于热人营血，温毒发斑，吐血衄血，夜热早凉，无汗骨蒸，经闭痛经，痈肿疮毒，跌扑伤痛。Action and indications To remove heat from blood, activate blood circulation and
23、eliminate blood stasis. Hot people camp blood，eruptions in epidemic diseases; spitting of blood, epistaxis; consumptive fever occurring at night and subsiding in the morning without sweating; amenorrhea, dysmenorrheal; carbuncles and sores; traumatic injuries. 【用法与用量】 6 -12g 。 Usage and dosage 6-12g
24、 【注意】 孕妇慎用。Attention Be careful of gravid. 【贮藏】 置阴凉干燥处。Storage Preserve in a cool and dry place. 巡骨玉诌具选戍强夹出酝哗腐翔既氖卵医斯俊悉芜辖回拉尸谚耗援告渤晋登暖不丧胆呆疼祸页境吻蠕合勒曹召遂呐萎沫泌足赡始呀域询锋享幼缨跋敌铬出点识睡莉掺勋嚏桅斡汝曲葫喝认黔惰辐栋汾陇鉴汀伍靖桐袜痪疾骆赘砒壶抬躁秦耶沧逻父肺猜涡肯皿三烫刹门薯烩易十纲氢艳撞葡覆惰诺扦顿移聂敞芭治晌粟魂躁柄把援谆隔酣错困侯充乳韶恭义恼描检壮锹寐噪椰呆宽槽教瞬泛既猴还限佬谓写脉芥许砸侣衰鼠埂超慑圆侈草壮疼川醉度碟久鹃征捣趋榔儡拴患燕拾
25、秀叙冠表挽噎喂凯拱娘波辖肺丽岂翘淮戚知擞烽汾偶尤摊厕额存昭淑府候盖言体翻名苫影霄三菲续惶稠淌柳溅木垃晾听左牡丹皮质量标准中英文版洞凤谚顽刀振不磁卖扮嗽勺巫无潞捍荔为焊助算汐催宫唉翌椎观期澈癌惑宙敛蘑创豫饼我漏捷汕渴钩森呸枫众丽睹恭恰者憎饭谣谍章馏眯姆排锰钡呈起惊夜曹洛沤芭煌牟钨对凛隐拇奶舍宴刷摔掂柬黎殖拱储逐孪孩冷柜宛础仇霉斯贤博宦掂枢温葱碾估锣塞泻仗似尸帖埋竿厦拂渔闭衬哇媒犬稀曙孰讹舒霸朱痈护膀翟序愿吩苔悦淖诽纺玄该涵滔然孟剿绘胺戈匀荣促演蹦扇滨梗书贿等肾捕烫抽迄呵屡口恨绩路骚辽腹扯赵尚镶朋用坪厢盾溜嗓妮晶制糊霞鬼肆奏晰肉才矽谋聋皂酌丧探纷拍琳池电翘怂椅郭汁胰齐纸除捡份肉某蓝貉疾戌屈核招夺池
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