精选优质文档-倾情为你奉上序号配体条件结构来源1ZrOCl2.8H2O (200 mg), H3TATB (60 mg) and 0.6mL trifluoroacetic acid in 12 mL of DEF were ultrasonically dissolved in a Pyrex vial. The mixture was heated at 120 C in an oven for 12 h. After cooling down to room temperature, white powder crystalline precipitate was harvested by filtrationPCN-777Angew. Chem. Int. Ed. 2014, 53, 1 72 All samples were synthesized via a reflux method involving the reaction of 2-sulfoterephthalic acid with Zr
